1. Heat potassium trixochlorate V in the presence of manganese iv oxide (as a catalyst) in the ratio 4:1 by mass in a hard test tube fitted with a delivery tube.
2. The oxygen gas produced from the mixture is passed through a U tube containing (anhydrous) calcium chloride to dry.
3. The issuing gas is collected over mercury in gas jar or test tube.
4. 2KCl03 (MnO2) → 2KCl + 3O2.
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